Assessment of Hot-Water-Alkali Treated Bagasse Fiber in Metakaolin-Based Geopolymer Using Machine Learning
DOI:
https://doi.org/10.46604/aiti.2026.15755Keywords:
geopolymer, metakaolin, bagasse fiber, hot-water-alkali treatment, machine learningAbstract
This study aims to develop metakaolin-based geopolymers reinforced with sugarcane bagasse fiber (BF) and to evaluate the effect of BF treatment on the composite's performance. The BF is pretreated with hot water and sodium hydroxide before being incorporated into the geopolymer matrix. Metakaolin-based geopolymer specimens containing 0%, 3%, 4%, and 5% BF by weight are prepared, and their mechanical properties and water absorption are analyzed. Scanning electron microscopy and Fourier transform infrared spectroscopy analyses reveal that the combined hot-water-alkali treatment significantly modifies the fiber surface. The treatment removes impurities and increases surface roughness, thereby enhancing fiber–matrix bonding. As a result, this treatment improves compressive and splitting tensile strength (STS) while reducing water absorption compared to untreated BF. Furthermore, machine learning algorithms, including random forest, AdaBoost, and XGBoost, are applied to predict STS. Among the three models, XGBoost demonstrates the highest predictive accuracy (R^² = 0.95, MAE = 0.28), indicating reliable predictions of mechanical strength.
References
H. H. Ahmad and Tavio, “Experimental Study of Cold-Bonded Artificial Lightweight Aggregate Concrete,” AIP Conference Proceedings, vol. 1977, article no. 030011, 2018.
D. Christianto, Tavio, and D. Kurniadi, “Effect of Steel Fiber on the Shear Strength of Reactive Powder Concrete,” IOP Conference Series: Materials Science and Engineering, vol. 508, article no. 012006, 2019.
Z. Zhang, L. Zhang, H. Liu, and J. Yin, “Effects of Metakaolin and Sodium Silicate Treatment on Highwater Content Dredged Clay for Improved Construction Fill Performance,” Construction and Building Materials, vol. 411, article no. 134196, 2024.
G. Sharmila and R. Jeyalakshmi, “Unravelling the Stability of Solvated Silicate Species in Sodium Silicate Activator Solution of Different Silica Modulus by FTIR and NMR Studies and Their Chemical Reactivity on Metakaolin and Fly Ash Geopolymerisation,” Sustainable Chemistry and Pharmacy, vol. 39, article no. 101578, 2024.
G. M. Amantino, N. P. Hasparyk, F. Tiecher, and R. D. Toledo Filho, “Assessment of Bio-Aggregate Concretes’ Properties with Rice Residue,” Journal of Building Engineering, vol. 52, article no. 104348, 2022.
H. M. Hamada, A. Al-attar, S. Beddu, M. Kamal, S. T. Yousif, and A. Majdi, “Impact of Rice Husk Ash on Geopolymer Concrete: A Literature Review and Future Directions,” Case Studies in Construction Materials, vol. 22, article no. e04476, 2025.
B. Kozub, S. Gądek, B. Tyliszczak, L. Wojnar, and K. Korniejenko, “Leveraging 3D Printing Capability for Geopolymer Composites Based on Fly Ash with Cotton Fibers Addition”, International Journal of Engineering and Technology Innovation, vol. 14, no. 3, pp. 231-243, 2024.
A. Workiye and E. Woldesenbet, “Porous Maize Stalk Cellulose Fiber-Reinforced Geopolymer Composites for Heat Insulation at the Bottom Side of a Local Electric Stove”, International Journal of Engineering and Technology Innovation, vol. 22, pp. 20-29, 2022.
R. N. Yanou, R. C. KAZE, A. Adesina, J. G. D. Nemaleu, S. B. K. Jiofack, and J. N. Y. Djobo, “Performance of Laterite-Based Geopolymers Reinforced with Sugarcane Bagasse Fibers,” Case Studies in Construction Materials, vol. 15, article no. e00762, 2021.
R. Y. Nkwaju, J. N. Y. Djobo, J. N. F. Nouping, P. W. M. Huisken, J. G. N. Deutou, and L. Courard, “Iron-Rich Laterite-Bagasse Fibers Based Geopolymer Composite: Mechanical, Durability and Insulating Properties,” Applied Clay Science, vol. 183, article no. 105333, 2019.
P. Rovnaník, “Effect of Curing Temperature on the Development of Hard Structure of Metakaolin-Based Geopolymer,” Construction and Building Materials, vol. 24, no. 7, pp. 1176-1183, 2010.
C. D. Atiş, E. B. Görür, O. Karahan, C. Bilim, S. Ilkentapar, and E. Luga, “Very High Strength (120 MPa) Class F Fly Ash Geopolymer Mortar Activated at Different NaOH Amount, Heat Curing Temperature and Heat Curing Duration,” Construction and Building Materials, vol. 96, pp. 673-678, 2015.
L. K. Turner and F. G. Collins, “Carbon Dioxide Equivalent (CO2-e) Emissions: A Comparison Between Geopolymer and OPC Cement Concrete,” Construction and Building Materials, vol. 43, pp. 125-130, 2013.
L. Prasad, S. Kumar, R. V. Patel, A. Yadav, V. Kumar, and J. Winczek, “Physical and Mechanical Behaviour of Sugarcane Bagasse Fibre-Reinforced Epoxy Bio-Composites,” Materials, vol. 13, no. 23, article no. 5387, 2020.
M. Djalal, M. Nafissa, R. Mansour, M. Jawaid, M. Hocine, and B. Lamia, “Effect of Alkali Treatment on New Lignocellulosic Fibres from the Stem of the Aster Squamatus Plant,” Journal of Materials Research and Technology, vol. 32, pp. 2882-2890, 2024.
M. Y. R. da Gloria, V. M. Andreola, D. O. J. dos Santos, M. Pepe, and R. D. Toledo Filho, “A Comprehensive Approach for Designing Workable Bio-Based Cementitious Composites,” Journal of Building Engineering, vol. 34, article no. 101696, 2021.
J. Cai, J. Pan, J. Han, and X. Wang, “Mechanical Behaviors of Metakaolin-Based Engineered Geopolymer Composite under Ambient Curing Condition,” Journal of Materials in Civil Engineering, vol. 34, no. 7, pp. 1-12, 2022.
L. Breiman, “Random Forests,” Machine Learning, vol. 45, pp. 5-32, 2001.
P. F. Zhang, M. Iqbal, D. Zhang, X. L. Zhao, and Q. Zhao, “Bond Strength Prediction of FRP Bars to Seawater Sea Sand Concrete Based on Ensemble Learning Models,” Engineering Structures, vol. 302, article no. 117382, 2024.
R. E. Schapire and Y. Freund, “Bodomosting: Foundations and Algorithms,” Kybernetes, vol. 42, no. 1, pp. 164-166, 2013.
M. H. R. Sobuz, M. H. Khan, M. K. I. Kabbo, A. H. Alhamami, F. S. Aditto, M. S. Sajib, et al., “Assessment of Mechanical Properties with Machine Learning Modeling and Durability, and Microstructural Characteristics of a Biochar-Cement Mortar Composite,” Construction and Building Materials, vol. 411, article no. 134281, 2024.
Y. Zeng, Y. Chen, Y. Liu, T. Wu, Y. Zhao, D. Jin, et al., “Prediction of Compressive and Flexural Strength of Coal Gangue-Based Geopolymer Using Machine Learning Method,” Materials Today Communications, vol. 44, article no. 112076, 2025.
W. Huo, Z. Zhu, H. Sun, B. Ma, and L. Yang, “Development of Machine Learning Models for the Prediction of the Compressive Strength of Calcium-Based Geopolymers,” Journal of Cleaner Production, vol. 380, part 2, article no. 135159, 2022.
S. M. Lundberg and S. I. Lee, “A Unified Approach to Interpreting Model Predictions,” Proceedings of Neural Information Processing Systems (NIPS’17), ACM Press, pp. 4768-4777, 2017.
X. Zhao, P. F. Zhang, Q. Zhao, D. Zhang, Y. Tuerxunmaimaiti, and H. Cao, “A SHAP Algorithm-Based Prediction of the Interlaminar Shear Strength Degradation of G/BFRP Bars Embedded in Concrete Exposed to Marine Environment,” Case Studies in Construction Materials, vol. 22, article no. e04770, 2025.
A. Bartos et al., “Alkali Treatment of Lignocellulosic Fibers Extracted from Sugarcane Bagasse: Composition, Structure, Properties,” Polymer Testing, vol. 88, article no. 106549, 2020.
Fahmida-E-Karim, M. R. Islam, P. Roy, M. Hasan, S. Islam, and S. Haque, “Analysis of Water Absorbency and Surface Behavior of Kapok and Bagasse Fibers After Alkali Treatment,” Cleaner Waste Systems, vol. 12, article no. 100357, 2025.
A. Workiye and E. Woldesenbet, “Flexural Strength and Porosity of NaOH-Treated Maize Stalk Cellulose-Fibers-Reinforced Geopolymer Composites”, International Journal of Engineering and Technology Innovation, vol. 25, pp. 44-53, 2023.
H. M. Hamada, A. Al-Attar, M. Kamal, S. Beddu, and A. Majdi, “Advancing the Sustainability of Fiber-Reinforced Geopolymer Concrete Using Natural Plant Fibers: A Comprehensive Review of Properties and Impacts,” Structures, vol. 77, article no. 109201, 2025.
B. Poletanovic, J. Dragas, I. Ignjatovic, M. Komljenovic, and I. Merta, “Physical and Mechanical Properties of Hemp Fibre Reinforced Alkali-Activated Fly Ash and Fly Ash/Slag Mortars,” Construction and Building Materials, vol. 259, article no. 119677, 2020.
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